Structure elucidation by NMR in organic chemistry : a practical guide / Eberhard Breitmaier
Tipo de material: TextoDetalles de publicación: Chichester : John Wiley & Sons, 2004 Edición: 3rd rev. edDescripción: XII, 258 p. : gráf. ; 24 cmISBN: 0-470-85007-8Tema(s): Espectroscopia de resonancia magnética nuclear | Compuestos orgánicos -- Espectroscopía | Química orgánicaResumen: A brief introduction gives an overview of the basic principles and elementary instrumental methods of NMR. This is followed by instructional strategy and tactical advice on how to translate spectra into meaningful structural information. The book provides the student with 55 sets of spectra of graduated complexity. These are designed to challenge the student's problem-solving abilities by the introduction of new concepts with each group of problems, followed by possible solutions and full explanations. A formula index of solutions is provided at the end of the text.This third edition, following on from the second (a reprint of the first edition with corrections), presents significant new material. Thus, actual methods of two-dimensional NMR such as some inverse techniques of heteronuclear shift correlation, as well as the detection of proton-proton connectivities and nuclear Overhauser effects are included. To demonstrate the applications of these methods, new problems have replaced those of previous editions.Resumen: INDICE: 1. Short introduction to basic principles and methods 2. Recognition of structural fragments by NMR 3. Problems 4. Solutions to problems. References. Formula index of solutions to problems. Subject index.Tipo de ítem | Biblioteca de origen | Signatura | URL | Estado | Fecha de vencimiento | Código de barras | Reserva de ítems | Bibliografía recomendada |
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Manuales | 02. BIBLIOTECA CAMPUS PUERTO REAL | 547:543.42/BRE/str (Navegar estantería(Abre debajo)) | Texto completo | Disponible Ubicación en estantería | Bibliomaps® | 3741453381 |
Indice
A brief introduction gives an overview of the basic principles and elementary instrumental methods of NMR. This is followed by instructional strategy and tactical advice on how to translate spectra into meaningful structural information. The book provides the student with 55 sets of spectra of graduated complexity. These are designed to challenge the student's problem-solving abilities by the introduction of new concepts with each group of problems, followed by possible solutions and full explanations. A formula index of solutions is provided at the end of the text.This third edition, following on from the second (a reprint of the first edition with corrections), presents significant new material. Thus, actual methods of two-dimensional NMR such as some inverse techniques of heteronuclear shift correlation, as well as the detection of proton-proton connectivities and nuclear Overhauser effects are included. To demonstrate the applications of these methods, new problems have replaced those of previous editions.
INDICE: 1. Short introduction to basic principles and methods 2. Recognition of structural fragments by NMR 3. Problems 4. Solutions to problems. References. Formula index of solutions to problems. Subject index.
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